INSTRUMENT CONTROL PARAMETERS: Ailent GCMS-2 ----------------------------------------------- Thu Feb 09 07:45:49 2023 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS Injection Location: Front Mass Spectrometer : Enabled No Sample Prep method has been assigned to this method. GC GC Summary Run Time 45 min Post Run Time 0 min Oven Temperature Setpoint On (Initial) 80 °C Hold Time 2 min Post Run 45 °C Program #1 Rate 5 °C/min #1 Value 280 °C #1 Hold Time 3 min Equilibration Time 2 min Max Temperature 325 °C Maximum Temperature Override Disabled Slow Fan Disabled ALS Front Injector Syringe Size 10 μL Injection Volume 1 μL Solvent A Washes (PreInj) 2 Solvent A Washes (PostInj) 2 Solvent A Volume 4 μL Solvent B Washes (PreInj) 2 Solvent B Washes (PostInj) 2 Solvent B Volume 4 μL Sample Washes 0 Sample Wash Volume 1 μL Sample Pumps 5 Dwell Time (PreInj) 0 min Dwell Time (PostInj) 0 min Solvent Wash Draw Speed 300 μL/min Solvent Wash Dispense Speed 3000 μL/min Sample Wash Draw Speed 300 μL/min Sample Wash Dispense Speed 3000 μL/min Injection Dispense Speed 6000 μL/min Viscosity Delay 0 sec Sample Depth 6 mm Injection Type Standard L1 Airgap 0.2 μL Solvent Wash Mode A, B Sample Overlap Mode Sample overlap is not enabled ALS Errors Pause for user interaction Front SS Inlet He Mode Splitless Heater On 230 °C Pressure On 9.6102 psi Total Flow On 26 mL/min Septum Purge Flow On 5 mL/min Septum Purge Flow Mode Switched Gas Saver On 15 After 2 min mL/min Purge Flow to Split Vent 20 mL/min at 0.75 min Liner A Liner has not been selected. Thermal Aux 2 (MSD Transfer Line) Temperature Setpoint On (Initial) 280 °C Column Column #1 Flow Setpoint Off (Initial) 1 mL/min Post Run 1 mL/min Column Information Agilent 19091S-433UI HP-5ms Ultra Inert Temperature Range -60 °C—325 °C (350 °C) Dimensions 30 m x 250 μm x 0.25 μm Column lock Unlocked In Front SS Inlet He Out MSD (Initial) 80 °C Pressure 9.6102 psi Flow 1 mL/min Average Velocity 36.62 cm/sec Holdup Time 1.3913 min Control Mode Constant Flow Column Outlet Pressure 0 psi Signals Signal #1: Test Plot Description Test Plot Save Off Data Rate 50 Hz Signal #2: Front Inlet Description Front Inlet Details Front Inlet Pressure Actual Save Off Data Rate 50 Hz Signal #3: Description None Signal #4: Description None MS Information -- ----------- General Information ------- ----------- Acquisition Mode : Scan Solvent Delay (minutes) : 4.5 Tune file : C:\MassHunter\GCMS\1\5977\etune.u EM Setting mode Gain : 1.000000 Normal or Fast Scanning : Normal Scanning Trace Ion Detection : Off Run Time (if MS only) : 10 minutes [Scan Parameters] Start Time : 4.5 Low Mass : 30 High Mass : 500 Threshold : 300 A/D Samples: : 4 [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C Timed Events ----- ------ Number Events= 0 END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US1930M034 --------------------------------- Trace Ion Detection is OFF. 34.593 : EMISSION 70.007 : ENERGY 0.503 : REPELLER 89.822 : IONFOCUS 17.627 : ENTRANCE_LENS 997.253 : EMVOLTS 1137.2 : Actual EMV 1.00 : GAIN FACTOR 2221.000 : AMUGAIN 135.313 : AMUOFFSET 2.000 : FILAMENT 1.000 : DCPOLARITY 12.357 : ENTLENSOFFSET 10.002 : Ion_Body -0.798 : EXTLENS -119.000 : MASSGAIN -24.000 : MASSOFFSET END OF TUNE PARAMETERS ---------------------- END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------